The Study of Drift in Inductively Coupled Plasma Optical Emission Spectrometry. Analysis of Silicate and Carbonate Raw Materials

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Title:The Study of Drift in Inductively Coupled Plasma Optical Emission Spectrometry. Analysis of Silicate and Carbonate Raw Materials
Creators:
Kanický, Viktor
Journal or Publication Title:
Collection of Czechoslovak Chemical Communications, 58, 12, pp. 2905-2917

Abstract

The work shows the importance of maintaining a constant temperature in a spray chamber to obtain a stable signal in the ICP spectrometry of water solutions. Simple shielding against ICP thermal radiation and forced air circulation in a plasma torch/spry chamber. The internal standard method has been used to improve signal stability. The number and composition of calibration solutions have been optimized for the detremination of the main constituents of some silicate and carbonate raw materials. An ultrasonic cleaning bath has been successfully used instead of stirring to dissolve the samples after fusion with LiBO<sub>2</sub>. Certified Czech and Slovak geological reference materials and some international standards have been used to test the accuracy. Statistical tests have proved that the method of determination complies with the requirements of technological standards.

Title:The Study of Drift in Inductively Coupled Plasma Optical Emission Spectrometry. Analysis of Silicate and Carbonate Raw Materials
Creators:
Kanický, Viktor
Divisions:Life and Chemical Sciences > Institute of Organic Chemistry and Biochemistry > Collection of Czechoslovak Chemical Communications
Journal or Publication Title:Collection of Czechoslovak Chemical Communications
Volume:58
Number:12
Page Range:pp. 2905-2917
ISSN:0010-0765
E-ISSN:1212-6950
Publisher:Institute of Organic Chemistry and Biochemistry
Related URLs:
URLURL Type
http://dx.doi.org/10.1135/cccc19932905UNSPECIFIED
ID Code:404
Item Type:Article
Deposited On:06 Feb 2009 17:00
Last Modified:06 Feb 2009 16:00

Citation

Kanický, Viktor (1993) The Study of Drift in Inductively Coupled Plasma Optical Emission Spectrometry. Analysis of Silicate and Carbonate Raw Materials. Collection of Czechoslovak Chemical Communications, 58 (12). pp. 2905-2917. ISSN 0010-0765

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