Synthesis of Alkyl 1,2-Dicyanopyrrolidino[1,2-f]phenanthridine-3-carboxylates

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Title:Synthesis of Alkyl 1,2-Dicyanopyrrolidino[1,2-f]phenanthridine-3-carboxylates
Creators:
Potáček, Milan
Topinka, Tomáš
Dostál, Jiří
Humpa, Otakar
Journal or Publication Title:
Collection of Czechoslovak Chemical Communications, 60, 7, pp. 1191-1195

Abstract

<p>Alkyl 1,2-dicyanopyrrolidino[1,2-<i>f</i>]phenanthridine-3-carboxyla tes <i>II</i> were prepared from 5-(alkoxycarbonylmethyl)phenanthridinium bromides <i>I</i> and fumaronitrile in the presence of triethylamine. The products <i>II</i> underwent spontaneous dehydrogenation to give pyrrolino[1,2-<i>f</i>]phenanthridines <i>III</i>. The structures of the products were determined by spectral methods (IR, NMR, MS).

Title:Synthesis of Alkyl 1,2-Dicyanopyrrolidino[1,2-f]phenanthridine-3-carboxylates
Creators:
Potáček, Milan
Topinka, Tomáš
Dostál, Jiří
Humpa, Otakar
Divisions:Life and Chemical Sciences > Institute of Organic Chemistry and Biochemistry > Collection of Czechoslovak Chemical Communications
Journal or Publication Title:Collection of Czechoslovak Chemical Communications
Volume:60
Number:7
Page Range:pp. 1191-1195
ISSN:0010-0765
E-ISSN:1212-6950
Publisher:Institute of Organic Chemistry and Biochemistry
Related URLs:
URLURL Type
http://dx.doi.org/10.1135/cccc19951191UNSPECIFIED
ID Code:816
Item Type:Article
Deposited On:06 Feb 2009 17:04
Last Modified:06 Feb 2009 16:04

Citation

Potáček, Milan; Topinka, Tomáš; Dostál, Jiří; Humpa, Otakar (1995) Synthesis of Alkyl 1,2-Dicyanopyrrolidino[1,2-f]phenanthridine-3-carboxylates. Collection of Czechoslovak Chemical Communications, 60 (7). pp. 1191-1195. ISSN 0010-0765

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